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SEM Gas Heating

Operando heating, biasing under environmental conditions

Enclosed Gas Heating Cell Inside the SEM

The SEM Gas Heating sample holder platform is designed to image gas-phase reactions and transformations at the microscale. Our patented precision-machined chip loading mechanism operates without screws, facilitating reproducible sample loading, self-aligning windows, stable imaging under gas flow up to 2 bar and heating beyond 1000 °C without the need for drift correction. This simplifies the hardware learning curve, workflows, and micrograph acquisition, guaranteeing reproducible sample preparation and in-situ SEM methodologies.

Advantages:

  • Custom-fitted stage and port hardware for any SEM
  • Fully user-replaceable PEEKSIL gas tubing for easy cleaning
  • Gas delivery systems with 1 to 8 channels plus dedicated purge line
  • Heating and gas delivery software with unlimited license for unrestricted experimentation  
  • Compatible with TEM, SEM, and X-ray microscopy workflows using cross-platform microfabricated chips.
  • Quick delivery of a broad selection of chip options for uninterrupted experimentation

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Designed for Advanced Nanoscale Gas-phase Dynamics Research

Advance fundamental understanding of heterogeneous catalysis performance and degradation, corrosion, thin film deposition and dissolution, nanoparticle dynamics, temperature-dependent reactions, and redox of nanostructures in a range of gaseous environments.

Understand Mechanisms Behind Gas-phase Transformations  

The transformations that occur at gas-solid interfaces are often microscale and highly transient, but nanostructure design and performance is highly dependent on the mechanisms that drive these transformations. The SEM Gas Heating sample holder applies stimuli such as temperature, electrical bias, light exposure, and gas composition and pressure changes to uncover reaction pathways, structural transformations, and degradation mechanisms to develop and characterize the next generation of functional catalysts, alloys and nanostructures.

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Technical Specs
1300 series – Single Channel
1300 Series – Multi-Channel
Pressure Range at Sample
1 to 2 bar
3–8, up to 1 vapor
Experimental Gas Inlets
1 on holder
10-6 mbar up to 2 bar
Purge Capability
Yes
Yes
Gas Analysis Capability
No
Yes
Tubing System
Metal and PEEKSIL
Metal and PEEKSIL
Biasing Contacts
4 contacts
4 contacts
Heating Temperature
>1000 °C
>1000 °C
EDS Compatible
Yes
Yes
TEM Compatibility
TFS/FEI, JEOL, Hitachi, Zeiss
TFS/FEI, JEOL, Hitachi, Zeiss
Instrument Type
SEM
SEM

Available For:

Key Features and Capabilities

Multi-channel gas delivery system

Unlock supreme control over your experimental gas composition with on-the-fly mixing and residual gas analysis

60+ In-Stock Gas-Cell SEM Chip Configurations

Keep experiments moving with in-stock gas-cell SEM chips designed for gas flow, heating, sample biasing, and multimodal microscopy workflows

SEM Safety & Seal Verification

Protect your SEM during gas-cell experiments and streamline setup with rapid high-vacuum seal checking.

Optimized for EDS

Perform correlative spectroscopy and microscopy for detailed in-situ elemental analysis

Multimodal Imaging

Correlate chemical, heating, biasing, and imaging data across TEM, SEM, and X-ray microscopy platforms

Single channel gas delivery system

Image samples in gas up to 2 bar using a sealed microfluidic chip assembly and pressure control system

Integrated Gas Heating

Add temperature-controlled gas-phase SEM capabilities with homogeneous heating, precise closed-loop temperature control and measurement beyond 1000 °C, and near-drift-free in-situ imaging

Reproducible Screw-Free Gas-Cell Assembly

Easy reproducible gas-cell assembly with self-aligning windows and a screw-free sealing design

Advanced Configuration Options